HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54417091, compound → HCID 20400830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54417091 | HCID 54417091 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Methane | HCID 297 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 20400830 | HCID 20400830 | — |
Reaction Steps
3-(7-Carboxyhept-6-enyl)-2-(3-pyridyl)-1-methylindole (100 mg) is dissolved in 10 ml of absolute ethanol with a catalytic amount of 10% palladium of charcoal and hydrogenated at 1 atmosphere pressure. After 1 mole of hydrogen is consumed, the catalyst is removed by filtration and washed with a few milliliters of ethanol. The combined filtrates are concentrated in vacuo to yield 3-(7-carboxyheptyl)-1-methyl-2-(3-pyridyl)indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04511573 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-53b6820e4e75492cb0839731bca88b72 |
| Source note | uspto-grants-1985_04 |