HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13424016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 13424015 | HCID 13424015 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 13424016 | HCID 13424016 | 118.1% |
Reaction Steps
Ethyl 1-(2-mesyloxyethyl)-3-carboethoxy-4-methylpyrrole-2-acetate (11.6 g) and 27 g of NaI was heated to reflux with 150 ml of acetonitrile for 1 hour. Solvent was removed by distillation and the residue triturated with water. The insoluble product was separated by filtration, air dried and crystallized from methylenechloride/hexane to yield 14.9 g of ethyl 1-(2-iodoethyl)-3-carboethoxy-4-methylpyrrole-2-acetate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04511724 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-7bb7fecf3e13467f8798de66ddb44aff |
| Source note | uspto-grants-1985_04 |