Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Isophorone | HCID 6544 | — |
| Reactant | Ozone | HCID 24823 | — |
| Product | 3,3-Dimethyl-5-oxohexanoic acid | HCID 11332610 | — |
Reaction Steps
A suspension of 15.8 g of isophorone in 110 ml of water was cooled down to 0° C. Then a stream of oxygen which contains about 4 percent of ozone was introduced until the suspension was saturated with ozone. The entire matter was now heated to 95° C. and was boiled for 3 hours under reflux. The 3,3-dimethyl-5-oxo-hexanoic acid was subsequently isolated by evaporation of water under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04511734 |
|---|
| Source dataset | uspto-grants-1985_04 |
|---|
| ORD ID | ord-a5f19b5596f74e3fbb8056938275b61b |
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| Source note | uspto-grants-1985_04 |
|---|
