HCID 20399854, compound → HCID 13472127, compound

Participants

Reaction Steps

A solution of the above 1-(6-methoxyhexanoyl)-1,2,3,4-tetrahydroquinoline (2.7 g) in ether (200 ml) containing lithium aluminium hydride (9.9 g) was refluxed for 6 hours, then cooled and diluted with water. The ethereal solution was dried and evaporated and the residue was chromatographed on silica gel, eluting with 99:1 methylene chloride:methanol, so as to obtain the title compound as an oil.

Provenance & Evidence