HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Phosphorus trichloride | HCID 24387 | — |
| Reactant | N'-acetyl-4-methoxybenzohydrazide | HCID 839858 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole | HCID 13054023 | — |
Reaction Steps
Using the procedure of Step B in Example 1, 26.3 ml of aniline, 150 ml of o-dichlorobenzene, 4.65 ml of phosphorus trichloride and 10 g of N-(4-methoxybenzoyl)-N'-acetyl-hydrazine [prepared by process of J.Org., Vol. 19 (1954), p. 194-201] were reacted to obtain 7.1 g of 3-(4-methoxyphenyl)-4-phenyl-5-methyl-4H-1,2,4-triazole melting at 140°-141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04512997 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-ae59bc73c42b40f0802da2ed801c8bc0 |
| Source note | uspto-grants-1985_04 |