Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-2-phenylpropanoic acid hydrochloride | HCID 20086446 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Methyl 2-amino-2-phenylpropanoate | HCID 14426739 | — |
Reaction Steps
A mixture of 4.3 g of methyl DL aminophenylpropanoate hydrochloride, 43 ml of demineralized water, 86 ml of ether and 3 ml of triethylamine was stirred at 20° C. for 10 minutes and the aqueous phase was extracted with ether. The combined ether phases were dried and evaporated to dryness under reduced pressure to obtain 8.3 g of methyl aminophenylpropanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04513139 |
|---|
| Source dataset | uspto-grants-1985_04 |
|---|
| ORD ID | ord-ec0bcd55ae48438697719f4415bf78fc |
|---|
| Source note | uspto-grants-1985_04 |
|---|
