HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine methyl ester → methyl Boc-D-methionyl-glycinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine methyl ester | HCID 69221 | — |
| Reactant | N-(tert-Butyloxycarbonyl)-D-methionine | HCID 111051 | — |
| Product | methyl Boc-D-methionyl-glycinate | HCID 13216971 | — |
Reaction Steps
The title compound was prepared by the general method of Preparation 1 using 198 g (0.79 mole) of t-butoxycarbonyl-D-methionine (Boc-D-Met) and 99.5 g (0.79 mole) glycine methyl ester (Gly-OMe) hydrochloride. The title compound was isolated as an analytically pure solid without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04514332 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-ec38b1c80d9a44fa95a13da3e549eb21 |
| Source note | uspto-grants-1985_04 |