1,1,5-Trichloro-3,3-dimethylpent-1-ene → HCID 13089648, compound

Participants

Reaction Steps

201.5 g (1 mol) of 3,3-dimethyl-1,1,5-trichloropent-1-ene were slowly added dropwise to 1,000 ml of quinoline at from 225° to 230° C., and distillate was taken off simultaneously via the top of the column. The temperature was increased until the quinoline boiled, and a total of 126 g of distillate were isolated and again fractionated. 121 g (73% of theory) of 1,1-dichloro-3,3-dimethyl-1,4-pentadiene of boiling point 49° to 53° C./20 mm Hg were obtained. ##STR25##

Provenance & Evidence