HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 13424177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,4-Diphenyl-3-butenyl bromide | HCID 10401774 | — |
| Reactant | Methyl 2-(pyrrolidin-3-yl)acetate | HCID 13424175 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13424177 | HCID 13424177 | — |
Reaction Steps
A mixture of 44.5 g. (0.138 mole) of methyl 3-pyrrolidineacetate hexamate, 40.3 g. (0.140 mole) of 4,4-diphenyl-3-butenyl bromide and 38.2 g. (0.276 mole) of potassium carbonate in 400 ml. of acetone was refluxed for 43 hours. The mixture was chilled, filtered, concentrated and chromatographed on silica gel to give methyl 1-(4,4-diphenyl-3-butenyl)-3-pyrrolidineacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04514414 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-d0595a07a7774f79a3edc79d4da0fed5 |
| Source note | uspto-grants-1985_04 |