HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 68115964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-Chloropurine riboside | HCID 93003 | — |
| Reactant | 9H-fluoren-9-amine hydrochloride | HCID 2724685 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68115964 | HCID 68115964 | 63.1% |
Reaction Steps
4.0 g of 6-chloropurine riboside, 3.79 g of 9-aminofluorene hydrochloride and 3.52 g of triethylamine are refluxed in 100 ml ethanol under nitrogen for 20 hrs. the solvent is evaporated to dryness and residue is treated with 100 ml of cold water. Precipitated solid is filtered and treated with 50 ml of methanol-chloroform (1:1) affording 3.8 g (63%) of N6 -fluorenyladenosine having a m.p of 210°-212° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593019 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-9f942efe969e400fbb2a6e6cf35cb70b |
| Source note | uspto-grants-1986_06 |