HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86740823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-Chloropurine riboside | HCID 93003 | — |
| Reactant | HCID 20204011 | HCID 20204011 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86740823 | HCID 86740823 | 63% |
Reaction Steps
A mixture of 2.97 g of 6-chloropurine riboside, 2.25 g of fluorenylmethyl amine and 1.31 g of triethylamine is refluxed in 70 ml of ethanol under nitroen for 20 hrs. Upon cooling, solid material crystallizes out which is filtered and retreated with boiling ethanol. Solid material obtained is filtered and dried affording 2.9 g (63%) of N6 -fluorenylmethyl adenosine having a melting point of 139°-142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593019 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-ff9bc81902ea46e99bcc411383fa3f08 |
| Source note | uspto-grants-1986_06 |