HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 13575826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 5,6-Dihydro-4H-pyrrolo[3,2,1-ij]quinoline-1,2-dione | HCID 2786143 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 13575826 | HCID 13575826 | 47.4% |
Reaction Steps
A mixture of 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-1,2-dione (7.49 g, 0.04 mole) and N-chlorosuccinimide (5.34 g, 0.04 mole) in carbon tetrachloride (40 ml) was refluxed for 23 hours. After cooling, the resultant red precipitate was collected by filteration, washed with water and dried. Recrystallization from acetonitrile afforded 4.2 g (47.4%) of red needles, melted at 188°-189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593092 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-6c4b9525bd1f46bfb8b54e8061cf280f |
| Source note | uspto-grants-1986_06 |