HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1981642Generated: November 3, 2026
Ammonia → Ethyl 2-acetamido-3-aminobut-2-enoate
https://huagongshe.com/reaction/1981642
Participants
| Role | Name | HCID | Charge |
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| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl 2-acetamido-3-oxobutanoate | HCID 224840 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 2-acetamido-3-aminobut-2-enoate | HCID 86740825 | — |
Reaction Steps
A solution of 0.054 mmol of ammonia in ethanol was added dropwise to 0.054 mol of ethyl 2-acetamidoacetoacetate in 40 ml of ice cold ethanol over a period of 10 minutes. The reaction vessel was tightly capped and allowed to stir overnight at 23° C., after which the solvent was removed at reduced pressure to provide ethyl 2-acetamido-3-aminobut-2-enoate in a 3/1 ratio of two geometrical isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04593118 |
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| Source dataset | uspto-grants-1986_06 |
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| ORD ID | ord-80c66047b6b5402985af6d7c529af9bf |
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| Source note | uspto-grants-1986_06 |
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