HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Diethylethylenediamine → HCID 13608033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Diethylethylenediamine | HCID 60993 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 13607992 | HCID 13607992 | — |
| Product | HCID 13608033 | HCID 13608033 | 33.1% |
Reaction Steps
Following the procedure of Example 16, N,N-diethyl aminoethylamine and 1,1'-carbonyldiimidazole and N,N-dimethyl-2-[4-[(3-piperidinyl)sulfonyl]phenoxy]ethanamine were reacted to give the title compound which was crystallized from diethyl ether-hexane as white crystals in 33.1% yield, m.p. 79°-80° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593102 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-dbe46b291e3f461081d7a5fed4bd74a8 |
| Source note | uspto-grants-1986_06 |