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HRID1981893

反应详情

EQUATION

反应方程式

HRID 1981893 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(C)I
HCID143426

Methyl 2-iodopropanoate

C4H7IO2

结构：CC(C)(C)OC(=O)NC1CSCCNC1=O
HCID15591256

Carbamic acid, (hexahydro-5-oxo-1,4-thiazepin-6-yl)-, 1,1-dimethylethyl ester

C10H18N2O3S

PRODUCTS

生成物

1
结构：COC(=O)C(C)N1CCSCC(NC(=O)OC(C)(C)C)C1=O
HCID23318043

未命名化合物

收率 81.5%

PROCEDURE

实验过程

The above-named compound is prepared from 6-t-butoxycarbonylamino-perhydro-1,4-thiazepin-5-one (0.1 g) and methyl iodopropionate (0.11 g) according to the procedure described in Example 4. The product (0.11 g) is obtained after chromatography. The NMR spectrum is consistent with the assigned structure.