HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86740840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 136332145 | HCID 136332145 | — |
| Reactant | HCID 136332146 | HCID 136332146 | — |
| Product | HCID 86740840 | HCID 86740840 | 83% |
Reaction Steps
In the same manner as described in Example 1 except that 2',5'-dihydroxy-6'-t-butylacetophenone oxime and thionyl chloride were used instead of 5'-t-butyl-2',4'-dihydroxyacetophenone oxime and phosphorus oxychloride, respectively, the desired 2-methyl-5-hydroxy-6-t-butylbenzoxazolol was obtained. Yield 83% (light brown needles), Melting Point 203° to 205° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04594426 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-504925b095af47669a6f225460fdb3e5 |
| Source note | uspto-grants-1986_06 |