HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxy-2,2-dimethylpropionic acid → HCID 23317293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxy-2,2-dimethylpropionic acid | HCID 78548 | — |
| Reactant | Propanedioic acid, 2-amino-, 1,3-diethyl ester | HCID 81272 | — |
| Product | HCID 23317293 | HCID 23317293 | 88% |
Reaction Steps
Diethyl N(β-hydroxypivaloyl)aminomalonate was prepared (method B) from β-hydroxy pivalic acid and diethyl aminomalonate in 88% yield. The compound was isolated as an oil. NMR 1.13-1.3 (12H, m), 3.5 (2H, br s), 4.16-4.4 (4H, q), 5.1-5.16 (1H, d), 7.6-7.7 (1H, d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595532 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-62626761337d4321b67e59f8c2686ff7 |
| Source note | uspto-grants-1986_06 |