HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-(Benzyloxy)-3-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | o-Vanillin | HCID 8991 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-(Benzyloxy)-3-methoxybenzaldehyde | HCID 1268087 | 98.8% |
Reaction Steps
50 g (0.3 mole) of 3-methoxysalicylaldehyde are heated to reflux for 3 hours with 51.3 g (0.3 mole) of benzyl bromide and 48.4 g of potassium carbonate in 300 ml of acetone. After filtration, the filtrate is concentrated. 71.8 g of the title compound are obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595685 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-dfe8a0ba1a0f4aa6a4347c8db1a1b032 |
| Source note | uspto-grants-1986_06 |