HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzaldehyde → HCID 2921732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | 6-Amino-1,3-dimethyluracil | HCID 81152 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 2921732 | HCID 2921732 | 13.6% |
Reaction Steps
A mixture of 6-amino-N,N'-dimethyluracil (3.1 g,20 mM),3-nitrobenzaldehyde (3 g,20 mM), and methyl acetoacetate (2.3 g, 1.4 ml, 20 mM) in glacial acetic acid (10 ml) was stirred under N2 at reflux for 3 hours, cooled to ambient, light yellow solid which was filtered and rinsed with acetone to give the title compound (1.04 g,13.5%),mp >230° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596805 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-15204affe4764727b228f8716ed2d003 |
| Source note | uspto-grants-1986_06 |