Acetic Anhydride → HCID 13669709, compound

HRID 1982401Notes

Reaction equation

HRID 1982401 reaction equation
[OH:1][CH2:2][CH:3]1[O:15][C:14]2[C:13]3[CH:12]=[CH:11][CH:10]=[N:9][C:8]=3[N:7]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[C:6](=[O:22])[C:5]=2[CH2:4]1.[C:23](OC(=O)C)(=[O:25])[CH3:24]>C1C=CC=CC=1>[C:23]([O:1][CH2:2][CH:3]1[O:15][C:14]2[C:13]3[CH:12]=[CH:11][CH:10]=[N:9][C:8]=3[N:7]([C:16]3[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=3)[C:6](=[O:22])[C:5]=2[CH2:4]1)(=[O:25])[CH3:24]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 13669707HCID 13669707, compound

Product 1

HCID 13669709HCID 13669709, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The product of Example 2 is refluxed with acetic anhydride in benzene, and the resultant product is recrystallized from isopropyl acetate to give the title compound, m.p. 207°-208° C.

Workup

  1. customthe resultant product is recrystallized from isopropyl acetate

Sources & evidence

ORD record
ord-49e16b446527436fb156660eea812115
Source dataset
uspto-grants-1986_06
Patent number
US04596809

Reaction notes

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