HCID 13669710, compound → HCID 13669708, compound

HRID 1982402Notes

Reaction equation

HRID 1982402 reaction equation
C([O:4][CH:5]1[CH2:18][O:17][C:16]2[C:15]3[CH:14]=[CH:13][CH:12]=[N:11][C:10]=3[N:9]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:8](=[O:25])[C:7]=2[CH2:6]1)(=O)C>CO>[OH:4][CH:5]1[CH2:18][O:17][C:16]2[C:15]3[CH:14]=[CH:13][CH:12]=[N:11][C:10]=3[N:9]([C:19]3[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=3)[C:8](=[O:25])[C:7]=2[CH2:6]1

Participants

3

Reactant 1

HCID 13669710HCID 13669710, compound

Product 1

HCID 13669708HCID 13669708, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrolysis of the product of Example 4 with methanol:1.0N sodium hydroxide solution followed by recrystallization of the resultant product from methanol yields the title compound, m.p. 296°-298° C.

Workup

  1. custom1.0N sodium hydroxide solution followed by recrystallization of the resultant product from methanol

Sources & evidence

ORD record
ord-b26e9092da654e1da75700189e14ff24
Source dataset
uspto-grants-1986_06
Patent number
US04596809

Reaction notes

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