HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → 5-(Bromomethyl)-2-pentyl-4-phenyl-1,3-oxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 5-Methyl-2-pentyl-4-phenyl-1,3-oxazole | HCID 23316595 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 5-(Bromomethyl)-2-pentyl-4-phenyl-1,3-oxazole | HCID 23316598 | — |
Reaction Steps
5-Methyl-2-pentyl-4-phenyloxazole (4.25 g) was brominated with N-bromosuccinimide (3.4 g) in carbon tetrachloride in the presence of azobisisobutyronitrile (0.2 g). The procedure gave an oil of 5-bromomethyl-2-pentyl-4-phenyloxazole, yield 5.70 g (99.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596816 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-bc81d66a0b11446d86671eebde14d4a8 |
| Source note | uspto-grants-1986_06 |