HCID 12923065, compound → HCID 23316728, compound

Participants

Reaction Steps

A mixture of 7.389 g (0.022 mol) of N-ethyl-N-heptyl-α-methyl-4-nitrobenzenebutanamine in 92 ml of ethanol was hydrogenated at room temperature overnight in the presence 0.74 g of 5% palladium-on-carbon. A total of 87% of theoretical hydrogen uptake was observed. The reaction mixture was filtered through Celite and the filtrate was evaporated to dryness under reduced pressure to provide 6.312 g of N-ethyl-N-heptyl-α-methyl-4-aminobenzenebutanamine as an oil.

Provenance & Evidence