HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-(4-Chlorophenyl)-5,6-dihydroimidazo[1,2-a]pyridine → Imidazo[1,2-a]pyridine,8-(4-chlorophenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-(4-Chlorophenyl)-5,6-dihydroimidazo[1,2-a]pyridine | HCID 13764023 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Imidazo[1,2-a]pyridine,8-(4-chlorophenyl)- | HCID 13764033 | — |
Reaction Steps
Combine 30 g (0.12 mol) of the product from Example 1 with 150 g of "activated" manganese dioxide in 500 ml of methylene chloride, and heat to reflux for 6 hr. Filter off the solids and remove the solvent in vacuo. The residue is crystallized from ether to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596872 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-9bbca1952d9c44b092c649958a95a177 |
| Source note | uspto-grants-1986_06 |