HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13764021, compound → HCID 13764031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13764021 | HCID 13764021 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13764031 | HCID 13764031 | — |
Reaction Steps
Combine 30 g (0.14 mole) of the product from Example 22 with 150 g of "activated" manganese dioxide in 500 ml of methylene chloride and heat to reflux for 6 hr. Filter the reaction mixture over celite, dry over magnesium sulfate, treat with charcoal, and remove the solvent in vacuo. Crystallize the residue from ether to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596872 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-692428075dfb4ea59e31d48dac6a844a |
| Source note | uspto-grants-1986_06 |