HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)phenol → HCID 13097729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)phenol | HCID 7376 | — |
| Reactant | 1-Bromomethylthio-4-chlorobenzene | HCID 13530086 | — |
| Product | HCID 13097729 | HCID 13097729 | 71% |
Reaction Steps
The synthesis was effected by reaction of 1-bromomethylthio-4-chlorobenzene and 3-trifluoromethylphenol in the same manner as described in preparation 3(b); yield 71%, b.p. 118°-122° C./0,01 mmHg. 1H NMR (CDC13); δ 5.13 (CH2), 7.1-7.5 (2×Ph), MS [70 eV 70, m/z (% rel. int)]: 318. (2,M), 159 (37), 157 (100), 145 (21) 121 (7), 108 (8), 75 (14)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596870 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-6e3389e0e19b4259b4e1c9af0d597589 |
| Source note | uspto-grants-1986_06 |