HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1982574Generated: November 2, 2026
Diketene → Butanoic acid, 3-oxo-, 2-phenoxyethyl ester
https://huagongshe.com/reaction/1982574
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diketene | HCID 12661 | — |
| Reactant | Phenoxyethanol | HCID 31236 | — |
| Product | Butanoic acid, 3-oxo-, 2-phenoxyethyl ester | HCID 12237326 | 40.8% |
Reaction Steps
Diketene (84 g) was added dropwise with stirring to 140 g of 2-phenoxyethanol heated at 100° C. After the addition was completed, the reaction mixture was refluxed for an additional 22 hours. The reaction mixture was fractionally distilled to obtain 90.6 g of 2-phenoxyethyl acetoacetate, BP 140°-145° C./0.3 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04596873 |
|---|
| Source dataset | uspto-grants-1986_06 |
|---|
| ORD ID | ord-23e94d4e94b5420793aae82081a6a23c |
|---|
| Source note | uspto-grants-1986_06 |
|---|
