HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54022822, compound → HCID 53751548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54022822 | HCID 54022822 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 53751548 | HCID 53751548 | 47.6% |
Reaction Steps
1.83 g (0.005 mol) (S)-1,1-dimethylethyl [[4-methyl-2-[[[5-methyl-2-thienyl]carbonyl]amino]pentyl]thio]acetate and 10 ml trifluoroacetic acid are reacted according to the procedure for Example 4 to give 0.75 g of (S)-[[4-methyl-2-[[(5-methyl-2-thienyl)carbonyl]amino]pentyl]thio]-acetic acid as a viscous oil. [α]D25 +57.3° (c 0.52, methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596819 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-11c9e71bd1024f809cefbd04c13a69c1 |
| Source note | uspto-grants-1986_06 |