2,4-Dichlorobenzyl alcohol → HCID 67527883, compound

HRID 1982897Notes

Reaction equation

HRID 1982897 reaction equation
Br[C:2]1[CH:3]=[N+:4]([O-])[CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9].[Cl:12][C:13]1[CH:20]=[C:19]([Cl:21])[CH:18]=[CH:17][C:14]=1[CH2:15][OH:16]>>[Cl:12][C:13]1[CH:20]=[C:19]([Cl:21])[CH:18]=[CH:17][C:14]=1[CH2:15][O:16][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9]

Participants

3

Reactant 2

HCID 156842,4-Dichlorobenzyl alcoholHCID 5485213-Bromo-4-nitropyridine N-oxide

Product 1

HCID 67527883HCID 67527883, compoundYield 68.2%

Procedure

In accordance with the same procedures as in Steps 3 and 4 of Preparation 1, except for using 3-bromo-4-nitropyridin-N-oxide prepared in Step 2 of Preparation 1 and 2,4-dichlorobenzyl alcohol, the titled compound was obtained (Yield: 68.2%).

Workup

  1. customIn accordance with the same procedures as in Steps 3 and 4 of Preparation 1

Sources & evidence

ORD record
ord-9b080d611eda4d8e9105f1d2f9ded133
Source dataset
uspto-grants-2009_06
Patent number
US07541366B2

Reaction notes

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