HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 23149209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23149195 | HCID 23149195 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23149209 | HCID 23149209 | — |
Reaction Steps
3.08 g of 3-formyl-1H-indole-1-ylmethanol was dissolved to 60 ml of dichloromethane. 2.5 ml of thionyl chloride was added to the solution, followed by stirring at room temperature for 3 hours. The reaction mixture was concentrated under reduced pressure to obtain 3.02 g of 1-(chloromethyl)-3-formyl-1H-indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541374B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-e3675aed2188421580116afc0d99ba7a |
| Source note | uspto-grants-2009_06 |