Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1983083Erstellt: 25. Oktober 2026

3-Methoxybenzoic Acid → HCID 16722534, Verbindung

https://huagongshe.com/reaction/1983083

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Methoxybenzoic AcidHCID 11461—
Edukt5-Methyl-3-phenyl-4-isoxazolecarbohydrazideHCID 727924—
ProduktHCID 16722534HCID 1672253467%

Reaktionsschritte

As described for example 2, 5-methyl-3-phenyl-isoxazole-4-carboxylic acid hydrazide (200 mg, 0.92 mmol) was converted using 3-methoxybenzoic acid instead of o-toluic acid to the title compound (SiO2, heptane:ethyl acetate=80:20 to 20:80, 205 mg, 67%) which was obtained as a white solid. MS: m/e=334.1 [M+H]+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07541372B2
Quelldatensatzuspto-grants-2009_06
ORD IDord-85b10863a35348c6856a252b8f479883
Quellennotizuspto-grants-2009_06