HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Methoxybenzoic Acid → HCID 16722534, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Methoxybenzoic Acid | HCID 11461 | — |
| Edukt | 5-Methyl-3-phenyl-4-isoxazolecarbohydrazide | HCID 727924 | — |
| Produkt | HCID 16722534 | HCID 16722534 | 67% |
Reaktionsschritte
As described for example 2, 5-methyl-3-phenyl-isoxazole-4-carboxylic acid hydrazide (200 mg, 0.92 mmol) was converted using 3-methoxybenzoic acid instead of o-toluic acid to the title compound (SiO2, heptane:ethyl acetate=80:20 to 20:80, 205 mg, 67%) which was obtained as a white solid. MS: m/e=334.1 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07541372B2 |
| Quelldatensatz | uspto-grants-2009_06 |
| ORD ID | ord-85b10863a35348c6856a252b8f479883 |
| Quellennotiz | uspto-grants-2009_06 |