化工社化工社 化学情報印刷レポート · 研究参考用
2-Methoxybenzoic acid → HCID 16722535、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methoxybenzoic acid | HCID 11370 | — |
| 反応物 | 5-Methyl-3-phenyl-4-isoxazolecarbohydrazide | HCID 727924 | — |
| 生成物 | HCID 16722535 | HCID 16722535 | 55% |
反応手順
As described for example 2, 5-methyl-3-phenyl-isoxazole-4-carboxylic acid hydrazide (200 mg, 0.92 mmol) was converted using 2-methoxybenzoic acid instead of o-toluic acid to the title compound (SiO2, heptane:ethyl acetate=95:5 to 50:50, 170 mg, 55%) which was obtained as a white foam. MS: m/e=334.0 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07541372B2 |
| 出典データセット | uspto-grants-2009_06 |
| ORD ID | ord-5caa5c4632204b6fa68f069463bc58ac |
| 出典メモ | uspto-grants-2009_06 |