HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methoxybenzoic acid → HCID 16722950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methoxybenzoic acid | HCID 2774545 | — |
| Reactant | HCID 67215709 | HCID 67215709 | — |
| Product | HCID 16722950 | HCID 16722950 | 31% |
Reaction Steps
As described for example 2, 5-cyclopropyl-3-phenyl-isoxazole-4-carboxylic acid hydrazide (1.32 g, 5.43 mmol) was converted using 4-fluoro-2-methoxy-benzoic acid instead of o-toluic acid to the title compound (SiO2, heptane:ethyl acetate:dichloromethane=70:10:20 to 40:40:20, 631 mg, 31%) which was obtained as a white solid. MS: m/e=319.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541372B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-959e3d088b3441cd8be69de45a9054cf |
| Source note | uspto-grants-2009_06 |