HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22261030, compound → HCID 22260751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22261030 | HCID 22261030 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ammonia | HCID 222 | — |
| Product | HCID 22260751 | HCID 22260751 | 141.5% |
Reaction Steps
By treating 17 mg of [3-(3-fluorophenyl)-1-(hydroxymethyl)-1H-5-indazolyl](2-thienyl)methanone, a by-product formed by incomplete deprotection in the above reaction, with concentrated aqueous ammonia solution in methanol, 11 mg of the title compound was further obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541376B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-3103ddc1ae0048a58f84dca647bd9de2 |
| Source note | uspto-grants-2009_06 |