HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopyridine → HCID 178421627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopyridine | HCID 7973 | — |
| Reactant | HCID 178418261 | HCID 178418261 | — |
| Reactant | HCID 178435098 | HCID 178435098 | — |
| Reactant | HCID 178461986 | HCID 178461986 | — |
| Product | HCID 178421627 | HCID 178421627 | — |
Reaction Steps
The title compound was prepared from the reaction of 2-(bicyclo[2.2. 1]heptan-2-ylamino)-5-methylthiazol-4(5H)-one with bromopyridine using the procedure described for 2a. 4.0 equivalent of LiN(SiMe3)2 was used. MS (ESI, pos. ion) m/z: 302 (M+1). % de (chiral LC): 20%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07541474B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-3ebd37d85cf34f468973ff80fe2375ef |
| Source note | uspto-grants-2009_06 |