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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1983637Generated: November 2, 2026

HCID 66758637, compound → HCID 86585735, compound

https://huagongshe.com/reaction/1983637

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66758637HCID 66758637—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
SolventEthyl AcetateHCID 8857—
ProductHCID 86585735HCID 8658573593.4%

Reaction Steps

To a solution of the product of example 274 (1.0 g) in methylene chloride(200 ml) was added manganese(IV) oxide(3.0 g), and the suspension was stirred at ambient temperature for 12 hours. The reaction mixture was diluted with ethyl acetate and filtered through celite. The solvent was evaporated under reduced pressure to give the titled compound(930 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07541365B2
Source datasetuspto-grants-2009_06
ORD IDord-85573f0cf7f14779a1dae89271a7c414
Source noteuspto-grants-2009_06