(2-Methoxyethyl)(methyl)amine → HCID 57713926, compound

HRID 1984044Notes

Reaction equation

HRID 1984044 reaction equation
Cl[S:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[NH:14][CH3:15])[C:8]([OH:10])=[O:9])(=[O:4])=[O:3].[CH3:16][O:17][CH2:18][CH2:19][NH:20][CH3:21]>>[CH3:16][O:17][CH2:18][CH2:19][N:20]([CH3:21])[S:2]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[NH:14][CH3:15])[C:8]([OH:10])=[O:9])(=[O:4])=[O:3]

Participants

3

Reactant 2

HCID 300977(2-Methoxyethyl)(methyl)amineHCID 57713890HCID 57713890, compound

Product 1

HCID 57713926HCID 57713926, compound

Procedure

3-(Chlorosulfonyl)-4-(methylamino)benzoic acid 1.2 was reacted with 2-methoxy-N-methylethanamine Ac following the procedure described in Example 1A to provide 1.3.Ac. MS analysis (m−1)=301.

Workup

  1. customto provide 1.3.Ac

Sources & evidence

ORD record
ord-49c6a785658948dd83789b14a74de759
Source dataset
uspto-grants-2009_06
Patent number
US07544676B2

Reaction notes

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