HCID 10249103, compound → HCID 11221281, compound

HRID 1984295Notes

Reaction equation

HRID 1984295 reaction equation
C[Sn](C)(C)[C:3]1[CH:4]=[C:5]2[CH2:11][C@:10]3([CH:16]4[CH2:17][CH2:18][N:13]([CH2:14][CH2:15]4)[CH2:12]3)[O:9][C:6]2=[N:7][CH:8]=1.FC(F)(F)S(O[C:27]1[C:35]2[C:30](=[N:31][CH:32]=[CH:33][CH:34]=2)[O:29][CH:28]=1)(=O)=O>>[O:29]1[C:30]2=[N:31][CH:32]=[CH:33][CH:34]=[C:35]2[C:27]([C:3]2[CH:4]=[C:5]3[CH2:11][C@:10]4([CH:16]5[CH2:17][CH2:18][N:13]([CH2:14][CH2:15]5)[CH2:12]4)[O:9][C:6]3=[N:7][CH:8]=2)=[CH:28]1

Participants

3

Reactant 2

HCID 10249103HCID 10249103, compoundHCID 58617644HCID 58617644, compound

Product 1

HCID 11221281HCID 11221281, compound

Procedure

Prepared by a method analogous to that described for the preparation of Example 1 from (2′R)-5′-trimethylstannyl-spiro[1-azabicyclo[2.2.2]octane-3,2′(3′H)-furo[2,3-b]pyridine] and furo[2,3-b]pyridin-3-yl trifluoromethanesulfonate. The title compound was obtained as a colourless solid; m/e 334 (MH+).

Workup

  1. customPrepared by a method analogous to

Sources & evidence

ORD record
ord-182c80b2fc10498eada9a7335124fdef
Source dataset
uspto-grants-2009_06
Patent number
US07544693B2

Reaction notes

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