HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethynyl-5-methyl-3-phenyl-isoxazole → HCID 24784181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethynyl-5-methyl-3-phenyl-isoxazole | HCID 53434647 | — |
| Reactant | HCID 178433060 | HCID 178433060 | — |
| Product | HCID 24784181 | HCID 24784181 | 13% |
Reaction Steps
As described for example 11c, 4-ethynyl-5-methyl-3-phenyl-isoxazole (73 mg, 0.40 mmol) was converted using (4-iodo-2-methyl-1H-imidazole instead of 2-chloro-4-iodopyridine) to the title compound (SiO2, heptane:ethyl acetate=95:5 to 0:100, 14 mg, 13%) which was obtained as a light brown solid. MS: m/e=264.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07544704B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-4bd51d9e088c4b09bf62ab0b5e0d10c2 |
| Source note | uspto-grants-2009_06 |