Methyl Anthranilate → HCID 57717920, compound

HRID 1984849Notes

Reaction equation

C[O:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[NH2:10].[C:12]([C:16]1[CH:41]=[CH:40][C:19]([O:20][C:21]2[CH:30]=[C:29]3[C:24]([CH:25]=[C:26]([C:37](Cl)=[O:38])[N:27]=[C:28]3[CH2:31][CH:32]3[CH2:36][CH2:35][CH2:34][CH2:33]3)=[CH:23][CH:22]=2)=[CH:18][CH:17]=1)([CH3:15])([CH3:14])[CH3:13]>>[C:12]([C:16]1[CH:41]=[CH:40][C:19]([O:20][C:21]2[CH:30]=[C:29]3[C:24]([CH:25]=[C:26]([C:37]([NH:10][C:5]4[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=4[C:3]([OH:2])=[O:11])=[O:38])[N:27]=[C:28]3[CH2:31][CH:32]3[CH2:33][CH2:34][CH2:35][CH2:36]3)=[CH:23][CH:22]=2)=[CH:18][CH:17]=1)([CH3:15])([CH3:13])[CH3:14]

Participants

Reactant 2

HCID 8635Methyl Anthranilate

HCID 86597133HCID 86597133, compound

Product 1

HCID 57717920HCID 57717920, compoundYield 57.4%

Procedure

The title compound (30 mg) was prepared following the same procedures that was described for example 432 from methyl-2-aminobenzoate (0.1 mmol, 15.1 mg) and 7-(4-tert-butyl-phenoxy)-1-cyclopentylmethyl-isoquinoline-3-carbonyl chloride (46 mg, 0.1 mmol).

Sources & evidence

ORD record: ord-7028071934724ff2a5033b5e87de2789
Source dataset: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07544699B2

Reaction notes

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