4-Phenylbenzyl chloride → HCID 10239178, compound

HRID 1985275Notes

Reaction equation

HRID 1985275 reaction equation
C[O:2][C:3](=[O:25])[C:4]([CH3:24])([O:6][C:7]1[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][CH2:15][CH:16]2[CH2:20][NH:19][C:18](=[O:21])[N:17]2[CH3:22])=[CH:9][C:8]=1[CH3:23])[CH3:5].[C:26]1([C:32]2[CH:39]=[CH:38][C:35]([CH2:36]Cl)=[CH:34][CH:33]=2)[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[C:32]1([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[CH:39]=[CH:38][C:35]([CH2:36][N:19]2[CH2:20][CH:16]([CH2:15][CH2:14][CH2:13][C:10]3[CH:11]=[CH:12][C:7]([O:6][C:4]([CH3:24])([CH3:5])[C:3]([OH:25])=[O:2])=[C:8]([CH3:23])[CH:9]=3)[N:17]([CH3:22])[C:18]2=[O:21])=[CH:34][CH:33]=1

Participants

3

Reactant 2

HCID 154634-Phenylbenzyl chlorideHCID 68867342HCID 68867342, compound

Product 1

HCID 10239178HCID 10239178, compound

Procedure

The titled compound was prepared using 2-Methyl-2-{2-methyl-4-[3-(3-methyl-2-oxo-imidazolidin-4-yl)-propyl]-phenoxy}-propionic acid methyl Ester (0.112 g, 0.322 mmole) and 4-phenyl benzyl chloride (0.078 g, 0.186 mmole) to produce an oil (0.054 g, 34%). Mass [EI+] 501 (M+H)+, [EI−] 499 (M−H)−.

Sources & evidence

ORD record
ord-1ad30e59ef5c476d8e41500e5c738cd6
Source dataset
uspto-grants-2009_06
Patent number
US07544812B2

Reaction notes

Loading…