4-Bromobenzyl bromide → HCID 10195963, compound

HRID 1985276Notes

Reaction equation

HRID 1985276 reaction equation
C[O:2][C:3](=[O:25])[C:4]([CH3:24])([O:6][C:7]1[CH:12]=[CH:11][C:10]([CH2:13][CH2:14][CH2:15][CH:16]2[CH2:20][NH:19][C:18](=[O:21])[N:17]2[CH3:22])=[CH:9][C:8]=1[CH3:23])[CH3:5].[Br:26][C:27]1[CH:34]=[CH:33][C:30]([CH2:31]Br)=[CH:29][CH:28]=1>>[Br:26][C:27]1[CH:34]=[CH:33][C:30]([CH2:31][N:19]2[CH2:20][CH:16]([CH2:15][CH2:14][CH2:13][C:10]3[CH:11]=[CH:12][C:7]([O:6][C:4]([CH3:24])([CH3:5])[C:3]([OH:25])=[O:2])=[C:8]([CH3:23])[CH:9]=3)[N:17]([CH3:22])[C:18]2=[O:21])=[CH:29][CH:28]=1

Participants

3

Reactant 2

HCID 685274-Bromobenzyl bromideHCID 68867342HCID 68867342, compound

Product 1

HCID 10195963HCID 10195963, compound

Procedure

The titled compound was prepared using 2-Methyl-2-{2-methyl-4-[3-(3-methyl-2-oxo-imidazolidin-4-yl)-propyl]-phenoxy}-propionic acid methyl Ester (0.100 g, 0.287 mmole) and 4-bromo benzyl bromide (0.108 g, 0.431 mmole) to produce an oil (0.058 g, 40%). Mass [EI+] 503, 505 (M+H)+, [EI−] 501, 503 (M−H)−.

Sources & evidence

ORD record
ord-78239171406543a29d375237480bbb48
Source dataset
uspto-grants-2009_06
Patent number
US07544812B2

Reaction notes

Loading…