Potassium Carbonate → HCID 22926256, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of 2.5 g of 4-cyclohexylphenol, 3.0 g of benzyl 2-bromoethyl ether and 2.4 g of potassium carbonate in N,N-dimethylformamide (50 ml) was stirred at 60° C. for 23 hours. The reaction solution was diluted with water and ethyl acetate. The organic layer was washed with saturated aqueous potassium carbonate and saturated ammonium chloride (×2), dried over anhydrous sodium sulfate and concentrated. The residue was purified by silica gel column chromatography, to give 3.9 g of the title compound as a colorless oil.

Provenance & Evidence