Ethylene Glycol → HCID 23005329, compound

HRID 1985429Notes

Reaction equation

HRID 1985429 reaction equation
[BH:1]([OH:3])[OH:2].[CH:4]([C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)=[O:5].[CH2:12](O)[CH2:13]O.[CH2:16](OCC)C>>[O:2]1[CH2:13][CH2:12][CH2:16][O:3][B:1]1[C:8]1[CH:7]=[C:6]([CH:11]=[CH:10][CH:9]=1)[CH:4]=[O:5]

Participants

4

Reactant 3

HCID 174Ethylene GlycolHCID 3283Diethyl EtherHCID 178519540HCID 178519540, compound

Product 1

HCID 23005329HCID 23005329, compound

Procedure

5.0 g of 3-Formylbenzene boronate was suspended in diethyl ether, and 3.7 ml of ethylene glycol was added, and the mixture was stirred at room temperature for 15 minutes. The solvent was concentrated, to give 10.36 g of the title compound as a colorless oil.

Workup

  1. concentrationThe solvent was concentrated

Sources & evidence

ORD record
ord-14838cef7bba4fa09372e922fff1b9b4
Source dataset
uspto-grants-2009_06
Patent number
US07544835B2

Reaction notes

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