HCID 69058861, compound → HCID 11997659, compound

Participants

Reaction Steps

To a solution of 0.014 g 2-cyclopropyl-5-methyl-5,6,7,8,8a,9-hexahydro-2H-2,4,4b,7-tetraaza-cyclopenta[b]fluorene in 1.0 ml glacial acetic acid and 1.00 ml water was added 0.005 g palladium 10% on charcoal and the mixture stirred for 18 h under 1 atmosphere of hydrogen at room temperature. The solvents were evaporated and the residue was purified by chromatography on silica gel with dichloromethane:methanol:ammonia=90:10:1 to yield 0.0025 g of the title compound as slightly brownish oil (MS: 271.3 (M+H+)).

Provenance & Evidence