HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 178516403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | HCID 178516237 | HCID 178516237 | — |
| Solvent | Propan-2-one--water (1/1) | HCID 18366337 | — |
| Product | HCID 178516403 | HCID 178516403 | 36% |
Reaction Steps
2,3-dihydroxypyridine (0.0027 mol), m-chloroaniline (0.0054 mol), and NaIO3 (0.0009 mol) were dissolved in 160 ml of water/acetone (80:1, v/v) solvent. The reaction mixture was stirred for 2 hours, and maintained still overnight. It was then filtered and recrystallized with chloroform. The final product was 5,6-di(m-chlorophenylamino)-2,3-pyridindione in a yellow powder. The yield was 36%-57%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547713B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-2b2bb8fcf63a4c808f51f544a29adffb |
| Source note | uspto-grants-2009_06 |