HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1985839Generated: October 29, 2026
HCID 57720229, compound → HCID 11168331, compound
https://huagongshe.com/reaction/1985839
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 57720229 | HCID 57720229 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11168331 | HCID 11168331 | 70.4% |
Reaction Steps
2-[3-(4-Benzyloxybutoxy)-4-phenylbenzylamino]-1-(β-D-ribofuranosyl)-1H-benzimidazole (35 mg) was dissolved in ethanol (5 mL). To the solution was added a catalytic amount of 10% palladium-carbon powder, and the mixture was stirred at 60° C. under a hydrogen atmosphere for 24 hour. The insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give the title compound (21 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07547680B2 |
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| Source dataset | uspto-grants-2009_06 |
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| ORD ID | ord-2e0967c0df824c9cb542375b886b782a |
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| Source note | uspto-grants-2009_06 |
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