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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1985839Generated: October 29, 2026

HCID 57720229, compound → HCID 11168331, compound

https://huagongshe.com/reaction/1985839

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57720229HCID 57720229—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 11168331HCID 1116833170.4%

Reaction Conditions

Temperature60 °C

Reaction Steps

2-[3-(4-Benzyloxybutoxy)-4-phenylbenzylamino]-1-(β-D-ribofuranosyl)-1H-benzimidazole (35 mg) was dissolved in ethanol (5 mL). To the solution was added a catalytic amount of 10% palladium-carbon powder, and the mixture was stirred at 60° C. under a hydrogen atmosphere for 24 hour. The insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give the title compound (21 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07547680B2
Source datasetuspto-grants-2009_06
ORD IDord-2e0967c0df824c9cb542375b886b782a
Source noteuspto-grants-2009_06