HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68845447, compound → HCID 57720186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68845447 | HCID 68845447 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57720186 | HCID 57720186 | 82.9% |
Reaction Steps
2-[3-(2-Carboxyvinyl)benzylamino]-1-(β-D-ribofuranosyl)-1H-benzimidazole (30 mg) was dissolved in methanol (2 mL). To the solution was added a catalytic amount of 10% palladium-carbon powder, and the mixture was stirred at room temperature under a hydrogen atmosphere for 1 hour. The insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give the title compound (25 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547680B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-6fc60aa2a6f44451b9cd904ede3ff970 |
| Source note | uspto-grants-2009_06 |