HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 57721399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 14449412 | HCID 14449412 | — |
| Reactant | HCID 22134479 | HCID 22134479 | — |
| Product | HCID 57721399 | HCID 57721399 | — |
Reaction Steps
Diacetylpyridine (1.43 g, 8.77 mmol and 4-eicosanoxy-3,5-diphenylaniline (9.5 g, 17.53 mmol) were dissolved in 400 ml of toluene. To this solution, 4 Å molecular sieves were added. After standing for 1 week, further 4 Å molecular sieves were added and the mixture was filtered. Most of the solvent was removed in vacuo. On standing a red precipitate was formed. The product, J, was isolated (5.52 g, 51%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547783B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-27caf230ccbc4d53961f1d09346f675b |
| Source note | uspto-grants-2009_06 |