2,6-Diacetylpyridine → HCID 57721388, compound

HRID 1986029Notes

Reaction equation

HRID 1986029 reaction equation
[CH3:1][C:2]1C=C(OCCCCCCCCCCCCCCCCCCCC)C(C(C)C)=C[C:3]=1N.[C:33]([C:36]1C=CC=C(C(=O)C)N=1)(=O)[CH3:34].[CH2:45]([O:65][C:66]1[CH:71]=[CH:70][C:69]([N:72]=[C:73]([C:75]2[CH:80]=[CH:79][CH:78]=[C:77]([C:81](=[N:83][C:84]3[CH:89]=[CH:88][C:87]([O:90][CH2:91][CH2:92][CH2:93][CH2:94][CH2:95][CH2:96][CH2:97][CH2:98][CH2:99][CH2:100][CH2:101][CH2:102][CH2:103][CH2:104][CH2:105][CH2:106][CH2:107][CH2:108][CH2:109][CH3:110])=[CH:86][C:85]=3[CH3:111])[CH3:82])[N:76]=2)[CH3:74])=[C:68]([CH3:112])[CH:67]=1)[CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][CH2:55][CH2:56][CH2:57][CH2:58][CH2:59][CH2:60][CH2:61][CH2:62][CH2:63][CH3:64]>C1(C)C=CC=CC=1>[CH3:112][C:68]1[CH:67]=[C:66]([O:65][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][CH2:55][CH2:56][CH2:57][CH2:58][CH2:59][CH2:60][CH2:61][CH2:62][CH2:63][CH3:64])[C:71]([CH:2]([CH3:3])[CH3:1])=[CH:70][C:69]=1[N:72]=[C:73]([C:75]1[CH:80]=[CH:79][CH:78]=[C:77]([C:81](=[N:83][C:84]2[CH:89]=[C:88]([CH:33]([CH3:36])[CH3:34])[C:87]([O:90][CH2:91][CH2:92][CH2:93][CH2:94][CH2:95][CH2:96][CH2:97][CH2:98][CH2:99][CH2:100][CH2:101][CH2:102][CH2:103][CH2:104][CH2:105][CH2:106][CH2:107][CH2:108][CH2:109][CH3:110])=[CH:86][C:85]=2[CH3:111])[CH3:82])[N:76]=1)[CH3:74]

Participants

5

Reactant 3

HCID 707902,6-DiacetylpyridineHCID 57721382HCID 57721382, compoundHCID 69036298HCID 69036298, compound

Product 1

HCID 57721388HCID 57721388, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The title compound was prepared by condensation of 2-methyl-4-eicosanoxy-5-isopropylaniline with 2,6-diacetylpyridine in the presence of 4 Å molecular sieves in refluxing toluene for 20 hours, similarly to the preparation of 2,6-bis[1-(4-eicosanoxy-2-methylphenylimino)ethyl]pyridine, described above.

Sources & evidence

ORD record
ord-ca25b339d6584494af18c6eed8122c45
Source dataset
uspto-grants-2009_06
Patent number
US07547783B2

Reaction notes

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